M ULT IPAGE 1 .

1 R:F 3CC O2H, S:H 2O, 30 min, 0°C

IMAGE
934473- 90-2 1 .2 R:NH3, S:H 2O, rt, neutralized

O O

H 2 N CH 2 C H 2 (C H 2 ) 4 N H C NH ( CH 2 ) 6 NH C NH
O

CH CH C NH CH 2

OH OH
HO O OH
CH 2 O H
O
O O O
HO HO CH2 OH
O
HO CH 2
O
HO CH2 OH OH
O O O
O

HO O OH
HO CH 2 OH OH
41 %

NO TE: Rea ct an ts : 1 , R ea ge nts : 2, S ol ve nt s: 1,

Ste ps : 1, S t age s: 2

Organic Letters, 9(6), 1053-1055; 2007

Bibliographic Information

Contraction of Supramolecular Double-Threaded Dimer Formed by  -Cyclodextrin with a

Long Alkyl Chain. Tsukagoshi, Shouichi; Miyawaki, Atsuhisa; Takashima, Yoshinori;
Yamaguchi, Hiroyasu; Harada, Akira. Department of Macromolecular Science, Graduate School
of Science, Osaka University, Toyonaka, Osaka, Japan. Organic Letters (2007), 9(6), 1053-
1055. Publisher: American Chemical Society, CODEN: ORLEF7 ISSN: 1523-7060. Journal
written in English. CAN 146:441990 AN 2007:196807 CAPLUS

Abstract
A double-threaded dimer bearing a long substituent part and a large stopper group has been
prepd. and showed a conformational change with increased solvent polarity.

http://pubs.acs.org/cgi-bin/article.cgi/orlef7/2007/9/i06/pdf/ol063078e.pdf