Patrick Isaiah A.

Talens 2013-19912 CATIONS Elimination Tests: Cation Cu2+ Fe3+ Zn2+ Ca2+ NH4+ +NaOH Blue ppt Orange/brown ppt White ppt White ppt NVR +xs NaOH Undissolved ppt Undissolved ppt Colorless soln Dissolved ppt Undissolved ppt NVR +NH3 Blue ppt Orange/brown ppt White ppt NVR NVR +xs NH3 Deep blue soln Dissolved ppt Undissolved ppt Colorless soln Dissolved ppt NVR NVR

Confirmatory Tests: Cation Cu2+ Fe3+ Zn2+ Ca2+ NH4+ Process 5 drops test soln + xs NH3 5 drops test soln + 2 drops 0.1 M KSCN 5 drops test soln + 2 drops K4Fe(CN)6 5 drops test soln + 2 drops K3Fe(CN)6 5 drops test soln + 2 drops K4Fe(CN)6 5 drops test soln + 2 drops 0.1 M (NH4)2C2O4 10 drops test soln + 5 drops 1 M NaOH Cover with watch glass with red & blue LP Observation Deep blue soln Blood red soln Dark blue ppt Yellow ppt White ppt White ppt Red->blue LP

ANIONS Elimination Tests: Anion CO3PO4SO4ISCNBrNO3+Ba(NO3)2 White ppt White ppt White ppt NR NR NR NR +FeCl3, HNO3, C7H8 Aq C7H8 +KMnO4, HNO3, C7H8 Aq C7H8

Pink Blood red

Pink Yellow

Confirmatory Tests: Anion Process CO35 drops test soln + 2 drops Ba(NO3)2 + 1M CH3COOH PO4SO4ISCNBrNO35 drops test soln + 2 drops Ba(NO3)2 + 1M CH3COOH 5 drops test soln + 2 drops Ba(NO3)2 + 5 drops 1M CH3COOH 5 drops test soln + 2 drops 1M HNO3 + 3 drops 0.1M FeCl3 + 5 drops C7H8 5 drops test soln + 2 drops 1M HNO3 + 3 drops 0.1M FeCl3 + 5 drops C7H8 5 drops test soln + 2 drops 1M HNO3 + 1 drop 0.1M KMnO4 + 5 drops C7H8 5 drops test soln + 1 drop 6M H2SO4 + 3 drops FeSO4 600 tt: + 2 drops 18M H2SO4 to side; slowly upright tt

Observation Ppt dissolution w/ effervescence Ppt dissolution w/o effervescence Undissolved ppt Pink C7H8 layer Deep red aq layer Yellow C7H8 layer Brown ring

5 drops test solution

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