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Elvi Dalgaard
P. Wanjara
8 PUBLICATIONS 21 CITATIONS
SEE PROFILE
SEE PROFILE
Xinjin Cao
John J. Jonas
McGill University
SEE PROFILE
SEE PROFILE
a
Materials Engineering, McGill University, 3610 University Street, Montreal, QC, Canada
Aerospace Manufacturing Technology Centre, Institute for Aerospace Research, National Research Council Canada, 5145 Decelles Avenue,
Montreal, QC, Canada
Abstract
The linear friction welding (LFW) behaviour of near-b titanium alloy Ti5Al5V5Mo3Cr (Ti-5553) was investigated by varying the
processing conditions of frequency and axial pressure. The examined mechanical properties of the welded material included microhardness
and tensile properties. The maximum strains experienced by the material during LFW for each set of welding parameters were estimated
based on the process parameters and then evaluated using Aramis, a three-dimensional optical deformation measurement system. The
LFWed Ti-5553 was examined with electron backscatter diraction techniques to relate the texture and phase changes to the
thermomechanical conditions. Characterisation of the welds included analysis of the microstructural features of the weld region and
the thermomechanically aected zone in relation to the parent material.
Crown Copyright 2011 Published by Elsevier Ltd. on behalf of Acta Materialia Inc. All rights reserved.
Keywords: Linear friction welding; Ti-5553; Microstructure; Tensile properties
1. Introduction
Beta (b) and near-b titanium alloys are of increasing
interest in the aerospace industry due to their better formability and toughness as compared with the more common
a+b Ti6Al4V alloy. High-strength metastable b alloys
such as Ti-5553 have potential to replace steel as the preferred material for large components such as the landinggear truck beam on the latest generation of airframes [1].
Ti-5553 was introduced in 1997 by TIMET and has the
nominal composition 5 wt.% Al, 5 wt.% V, 5 wt.% Mo,
3 wt.% Cr, with the balance being Ti. Table 1 lists some
typical physical and mechanical properties of this alloy in
the solution treated and aged (STA) condition. The forging
behaviour of Ti-5553 is similar to that of Ti10V2Fe3Al
(Ti1023), though the higher b transus temperature of
the former (856 C) vs. the latter (800 C) allows higher
forging temperatures [2].
Corresponding author at: Materials Engineering, McGill University,
3610 University Street, Montreal, QC, Canada.
E-mail address: ecdalgaard@gmail.com (E. Dalgaard).
1359-6454/$36.00 Crown Copyright 2011 Published by Elsevier Ltd. on behalf of Acta Materialia Inc. All rights reserved.
doi:10.1016/j.actamat.2011.04.037
856
4650
112
113
1236
1174
13
Frictional
Pressure
Stationary
(Top)
H Reciprocal
Motion (Bottom)
W
771
Horizontal
Fig. 1. Sample geometry and oscillation direction [6].
The equipment used for welding was an MTS LFW process development system, comprised of two hydraulic actuators: the in-plane actuator that oscillates the lower work
piece horizontally; and the forge actuator that applies a
downward load through the top stationary workpiece.
The technical specications of the equipment are described
elsewhere [6]. Table 2 shows the experimental plan used in
this study as well as the calculated maximum strain rate
using the equation proposed by Vairis and Frost [15], the
measured welding time and the total maximum strain calculated from these two latter quantities. The baseline
(BL) values of fBL (frequency) and PBL (pressure) were
established based on optima reported for Ti6Al4V [6],
since there is little in the literature regarding the friction
welding of b or near-b Ti alloys and no specic parameters
have been published [16]. Forging pressure was maintained
at the same level as during oscillation in order to examine
the eect of oscillation on the growth of the HAZ without
the complication of expelling extra material during the
forging phase. In general the a and b phase content of a
Ti alloy is very pertinent to its properties and hence to
the selection of thermomechanical processing parameters.
In LFW, the welding behaviour is closely related to the
ow stress; in the case of Ti-5553, since the material is
already mainly b phase, the use of parameters which led
to ow in the b phase of the Ti6Al4V material [6] was felt
to be valid (since thermomechanical processing would
occur in the b phase in any case). Ti-5553 material in ingot
form was sectioned to obtain weld coupons of 13 mm in
Table 2
Samples prepared.
Sample Frequency
ID
Pressure
LFW-1 fBL
PBL
3.6
LFW-2 Low (0.6fBL) High (1.5PBL) 2.2
1.3
1.6
4.8
3.5
772
grain boundary
(a)
(b)
Fig. 3. Parent material showing (a) a dark-eld image of the large equiaxed grains (Krolls reagent) and (b) high magnication backscatter electron image
of acicular substructure using compositional contrast (mirror polished).
773
Fig. 4. (a) As-welded LFW-1 showing (b) right and (c) left side ash cross-sections.
To reveal the details of the weld microstructure, including delineation of the grain boundaries and phase divisions,
orientation data were obtained from the as-received and
LFWed samples. Fig. 6 depicts the inverse pole gure
and phase fraction map of the as-received material, revealing that grains are equiaxed and 100250 lm in diameter.
Also observed is that the a phase comprises approximately
3% of the surface, and by extension, volume of the material. This phase is mainly concentrated at grain boundaries.
In order to improve the accuracy of the phase fraction
data, points in the scan with a condence index below 0.2
were discarded before calculation.
In Fig. 7, an inverse pole gure map of sample LFW-1
can be seen. An image quality map is overlaid in order to
dene the grain boundary locations. Clearly, in the aswelded condition, this alloy undergoes complete dynamic
recrystallization in the weld zone (200 lm wide) under
the thermomechanical conditions employed, namely the
combination of straining at elevated temperatures and high
strain rates. Beyond the weld region, an abrupt transition
to a thermomechanically aected zone (TMAZ) consisting
of mixed recrystallized and deformed grains is observed,
followed by a further transition to the original large b
grains. While the large equiaxed and deformed grains display a variety of orientations, it can be seen that, within
the recrystallized zone, the grains are predominantly oriented with their h1 1 1i directions normal to the sample surface. This represents the weld oscillation direction. This
reorientation to a preferred texture may be due to the
alignment during oscillation of the primary slip system in
this phase, {1 1 0}h1 1 1i, to be parallel with the oscillation
direction.
Fig. 8 indicates an overall phase area fraction of 0.4% a
in sample LFW-1. The a fraction decreases to nearly none
(estimated at 0.05%) in the recrystallized weld zone. This is
in contrast to the 3% a observed in the as-received material,
and indicates that the fast cooling rate experienced by the
material did not permit an equilibrium phase fraction to
774
(a)
(b)
grain boundary
(c)
(d)
Fig. 5. LFW-1 (Krolls reagent): (a) weld centre at high magnication, (b) 100 lm from weld centre, (c) 400 lm from weld centre, and (d) 1 mm from weld
centre.
Fig. 6. EBSD maps of as-received Ti-5553: (a) inverse pole gure map; (b) phase fraction map.
HAZ
TMAZ
Weld Center
TMAZ
775
HAZ
240 m
Fig. 8. Phase fraction map of LFW-1; points with condence index below 0.2 removed.
TMAZ
Weld Center
Fig. 9. Inverse pole gure of LFW-2 showing one side of weld zone with adjacent deformed grains.
In Fig. 12, b pole gures are presented for the recrystallized regions of LFW-1 and LFW-2. No a pole gures are
presented due to the negligible amount of a phase observed
in the material. The texture intensity of these recrystallized
zones can be seen to be very high, approximately 1015
times random. This strong texture is based on a large
776
Fig. 10. LFW-2 phase map; step size 2 lm; points with condence index below 0.2 removed.
Fig. 11. High-resolution scan of equiaxed grain zone at step size 0.10 lm: (a) inverse pole gure combined with image quality map; (b) phase map.
777
Fig. 12. b Pole gures of the recrystallized zones in (a) LFW-1; (b) LFW-2. The welding direction (WD) is normal to the gure (not shown); TD indicates
the direction transverse to WD, and ND the direction normal to the welding plane.
Fig. 13. Microhardness prole across the weld line for sample LFW-1
(baseline pressure and frequency).
Fig. 14. Microhardness prole across the weld line for sample LFW-2
welded at low frequency and high pressure.
Table 3
Tensile testing results.
As-received
LFW-1
LFW-2
YS (MPa)
UTS (MPa)
1046 13
1019 19
988 16
1108 25
1058 23
1013 10
7.4 3.0
3.0 0.5
2.0 0.1
11.2 6.5
4.0 1.0
2.9 0.9
778
(a)
Fracture surface
WZ
Fracture surface
WZ
Fig. 15. SEM images of fracture surfaces: (a) as-received, low magnication; (b) welded, low magnication; (c) as-received, high magnication; (d) welded,
high magnication.
(b)
Fig. 16. Polarized light micrographs of fractured tensile bars: (a) LFW-1
and (b) LFW-2.
at higher pressure and lower frequency, with LFW-1 displaying higher YS and UTS as well as greater elongation
(see Table 3). The better mechanical performance of
LFW-1 as compared to LFW-2 can be attributed to the
smaller amount of material aected thermomechanically
(weld zone and TMAZ), as indicated by the EBSD maps.
The fracture surfaces of the welded tensile coupons
revealed very large grains (see Fig. 15) that are consistent
with fracture occurring in the TMAZ adjacent to the
recrystallized weld zone. Both unwelded and welded samples displayed ductile fracture characteristics with some
areas of shear. In fact, all welded specimens fractured in
the TMAZ within 1 mm of the weld zone, as shown in
Fig. 16. Conversely, as-received (unwelded) tensile specimens fractured at random locations along their gauge
lengths. The consistent failure of the welded samples in
the TMAZ is most likely due to a depletion in the
coarse-grained microstructure, which would have a tendency to be weaker than the similarly depleted ne-grained
recrystallized weld zone.
An example of the strain distribution in the unwelded
condition is presented in Fig. 17. This should be compared
with that of the welded LFW-1 in Fig. 18. The region of
strain concentration indicated as the area of highest intensity in the welded specimen corresponds to the location of
the fracture that occurred immediately afterward. While it
779
Weld Line
TMAZ
TMAZ
PM
PM
780
Acknowledgements
The authors are grateful to Standard Aero Limited for
the materials used in this study. Thanks are also due to
M. Guerin, X. Pelletier and D. Chiriac for extensive technical assistance.
References
[1] Jones NG, Dashwood RJ, Dye D, Jackson M. Metall Mater Trans A
2009;40A:194454.
[2] Fanning JC. J Mater Eng Perform 2005;14(6):78892.