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Abstract
CO2-based EOR technology has been proven as an effective method to enhance light-oil recovery, while
to reduce CO2 emission. Miscible and near-miscible CO2 flooding have been extensively studied and
commercially applied in the past several decades; while CO2 huff-n-puff process did not gain too much
attention. CO2 huff-n-puff process may have better performance than CO2 flooding for a low-pressure
reservoir, in which reservoir pressure is far below the minimum miscible pressure (MMP), since the CO2
injection is able to build up the reservoir pressure, and the increased reservoir pressure will enhance the
mass transfer between the CO2 phase and the oil phase.
In this paper, 8 coreflood tests, totally 35 runs, are conducted to investigate the major factors affecting the
performance of CO2 huffnpuff in a low-pressure reservoir. The coreflood tests are conducted in a 984
mm-long composite core with an average porosity of 19.6% and an average permeability of 117 mD. The
reservoir pressure is 6.58 MPa, far below the measured MMP value of around 23 MPa. The effects of primary
operational parameters, such as CO2 injection rates, slug size, soaking time, injection pressure, pressure
depletion rates, and chasing gas (N2) on the huffnpuff performance have been extensively studied.
The experimental results indicate that the recovery factor for each cycle is reduced to 40% to 60%,
compared with that of the previous cycle. The recovery factor in each cycle is mainly affected by the total gas
slug size injected and the maximum pressure built up by gas injection. Chasing CO2 with N2 can effectively
reduce the CO2 usage, while increase the reservoir pressure to an ideal level, so that the maximum value of the
amount of the oil as recovered by per unit of CO2 injected can be obtained. It is also found that a long soaking
period is necessary to achieve a favorable performance while a long soaking time may greatly decrease the
average oil production rate of a cycle. In this study, it was observed that the first cycle rather than two cycles
following it was more sensitive to a long soaking time. The results of this study indicate that CO2 huff-n-puff
process has potential to rapidly improve the single-well performance in low-pressure reservoirs.
1. Introduction
Greenhouse gases (GHG) emissions are commonly identified as a major contributor to global warming.
CO2-based enhance oil recovery (EOR) techniques have shown great potential to recover remaining oil
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in secondary or tertiary production while offset the GHG emissions by means of sequestrating CO2
underground. CO2 flooding and cyclic CO2 injection (CO2 huff n puff), are two widely applied
CO2-based EOR techniques. The applicability of either EOR techniques mainly depends on reservoir
conditions, reservoir fluids, formation properties, and the availability of CO2 sources.
This study targets at a reservoir located in northwestern China with a very low original pressure of 12.9
MPa, far below its measured MMP value of 23 MPa. In addition, the reservoir formation is very tight,
permeability averaged 2.3 mD, in some regions even as low as 0.978 mD. The original reservoir pressure
is so low that there is no sufficient energy for the reservoir to do primary production. Furthermore,
waterflooding, a popular EOR method across the world, is not an option for this reservoir because of its
quite low permeabilities. The injectivity required by a successful waterflooding is not achievable.
However, for CO2 injection, injectivity problems do not exist. Additionally, there are abundant CO2
sources from large-scale coal chemical plants in the neighborhood of the reservoir and available for CO2
EOR use. Considering that CO2 flooding is not applicable in low-pressure reservoirs because of its poor
performance when an operation pressure is far below the corresponding MMP, CO2 huff-n-puff process
is a rational option.
CO2 huff-n-puff process is a typical single well operation, which was presented as an alternative of
cyclic steam stimulation for enhanced oil recovery (Stright et al., 1977; Patton et al., 1982; MongerMcClure et al., 1991). This process involves the injection of a slug of CO2, followed by a soaking time
allowing gas phase to mix with oil phase in place. Following the soaking time, the well is put into
production. The efforts to investigate the applicability of this process to enhance oil recovery have been
made for several decades with encouraging results. The results of laboratory tests and field treatments
demonstrated that CO2 huff-n-puff process is economically viable in diverse reservoir conditions.
Khatib et al. (1981) reviewed results of previous cyclic coreflood tests and field applications on
miscible CO2 injection and indicated that the use of CO2 is applicable in both heavy and light crude
to enhance oil recovery. Sayegh and Maini (1984) evaluated a huff-n-puff process in a Lioyminster
heavy oil reservoir by performing corefloods using CO2 and recycled produced gases. They
conducted an evaluation of relative permeabilities to gas and water at reservoir conditions as well as
an assessment of the longitudinal distribution of CO2 and the effect of soak period. On the basis of
field-treatment evaluations, Patton et al. (1982) and Haskin and Alston (1989) developed two
correlations to predict the process performance and some criteria to evaluate the extent to which how
a cyclic CO2 injection process is successful. One important economic indicator presented of
successful implementations is CO2 utilization, defined as the volume of CO2 used for per unit volume
of incremental oil produced, in unit of Mscf/STB. Its favorable rang is from 0.5 to 0.8 Mscf/STB.
Monger-McClure and her colleagues developed extensive research works on the feasibility of CO2
huff n puff process on light-oil recovery (Monger-McClure and Coma, 1988; Thomas et al., 1990;
Monger-McClure et al., 1991; Thomas and Monger-McClure, 1991). They investigated the influence
of various critical parameters, including CO2 slug size, the number of cycles, operational pressures,
impurity of CO2, reservoir gas, and gravity segregation and remaining oil saturation, by conducting
laboratory coreflood tests on watered-out cores in conjunction with comprehensive reviews of
hundreds of field applications. It was suggested that light-oil recovery by CO2 huff-n-puff either in
pressure-depleted reservoirs or for waterflood residual oil is promising. In addition, they also
compared the recovery mechanisms between CO2 injections on light-oil with heavy-oil. Torabi and
his team member investigated the performance of CO2 huff-n-puff process in naturally fractured
reservoirs by conducting experimental and simulation studies (Torabi and Asghari 2010; Torabi et al.
2012). Even though the volume ratio between fracture and matrix used in their laboratory model were
much larger than that in real reservoir scenarios, their research work filled the lack of information
relevant to the application of CO2 huff-n-puff process in naturally fractured reservoirs.
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Desity @ 20C
Average Molecular Weight
C11 Molecular Weight
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7.45
823.6
1.1458
67.2
2.60
Pb
(MPa)
Density @ Pb
(kg/m3)
Viscosity @ Pb
(cP)
Swelling factor
23.18
37.24
41.18
59.96
64.65
67.13
10.75
11.95
12.18
15.88
21.30
25.25
814.9
813.4
805.2
803.0
792.0
785.1
1.20
0.99
0.82
0.63
0.50
0.42
1.0616
1.1402
1.1792
1.3427
1.4932
1.5624
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Prosodity
(%)
Temperature
(C)
Pressure
(MPa)
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Table 5Conditions of CO2 huff-n-puff corefloods @ 44C (with a pressure drop of 0.5 MPa across the core)
to model a reservoirs closed outer boundary frequently encountered in field cases. The reservoir boundary
condition modeled in this study was different from those by previous literatures (Monger-McClure and
Coma, 1988; Thomas et al., 1990; Monger-McClure et al., 1991; Bardon et al., 1994; Shayegi et al., 1996;
Zhang et al., 2006), where a constant reservoir boundary with an aquifer was involved.
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11.37
5.35
4.85
4.05
13.96
9.25
8.64
8.4
7.69
13.48
8.89
8.21
7.89
7.39
13.33
9.04
8.42
8.61
7.51
11.37
11.37
11.37
11.37
11.37
11.37
11.37
11.37
11.37
11.37
8.15
6.88
12.34
11.74
10.86
12.58
14.28
5.7
3.48
0.7
15.91
7.49
4.63
2.42
1.08
13.78
7.06
4.59
2.46
0.89
16.17
8.48
4.87
2.21
1.17
9.47
7.06
4.76
11.37
1.13
10.2
7.43
4.78
2.91
1.34
7.7
4.62
5.01
8.32
6.33
4.15
24.16
Test 2
31.53
Test 3
28.78
Test 4
32.9
Test 5
24.8
Test 6
26.66
Test 7
17.33
Test 8
18.80
First, each core was completely saturated with formation water to measure its pore volume. Then, the
recombined oil was pumped into the core till no additional water produced to establish the original oil
saturation and connate water saturation. The core saturated with oil underwent subsequently a process of
aging to re-establish its wettability. All those operations occurred at reservoir conditions (5.68 MPa and
44C). Compared with the huff-n-puff corefloods by other researchers (Monger-McClure and Coma,
1988; Thomas et al., 1990; Monger-McClure et al., 1991; Bardon et al., 1994; Shayegi et al., 1996; Zhang
et al., 2006), the saturated core with oil in this study was not flooded again with formation water since
here CO2 huff-n-puff process was applied at the primary stage of production.
Once oil saturation and connate water saturation were established, the cyclic CO2 displacement process
was initiated by injecting gases from a compressed gas cylinder connected to the core injection end at a
constant injection rate measured at reservoir temperature of 44Cand ambient pressures. When the
designed amount of gases was completely pumped into the core, the gas injection (huff portion) ceased.
The injected gas slug was designed so that the core pressure was built up to a desired level. When chase
gas involved in the corefloods, it was injected after CO2 injection. Upon the cessation of gas injection, the
core was shut in for a period of time (soak period). Then, the core was returned to production (puff
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portion) from the injection end of the core while the other end was being closed. The production stage was
terminated when core pressure depleted to a certain level. The produced fluids were routed to the three
phase separator where oil phase and gas phase were permitted to separate. The produced oil was weighed
and its volume was calculated from the density of the dead oil. Once the volume of produced oil was
gained, the recovery factor for each cycle and the ultimate recovery factor for a whole test were calculated
from the volumetric material balance. The produced gas was routed into a gas meter to be measured there.
Obviously, the production process in this study was a pressure-depletion process, which was also different
from other studys operational pressure of a constant value during the production process (MongerMcClure and Coma, 1988; Thomas et al., 1990; Monger-McClure et al., 1991; Bardon et al., 1994;
Shayegi et al., 1996; Zhang et al., 2006). This injection-soaking-production process described above is one
typical huff-n-puff cycle.
A second cycle of gas injection was carried out immediately after the first cycle oil production ceased
and a third cycle conducted after the second one and so on. The same procedures were repeated in the
subsequent cycles in the similar manner to the first one with an exception that, in some cases, different
slug sizes of gases were injected. Upon the completion of a test, the core was cleaned carefully using the
same procedure described by Monger and Coma (1988) but petroleum ether rather than xylene was used
as cleaning liquid according to relevant Chinese regulations.
During the huff phase, pressure was gradually built up from the original reservoir pressure of 6.58 MPa
to the expected level while during the puff phase, the core pressure was depleted at a constant depletion
rate, 3- or 1.5 MPa/h, from the maximum pressure to a designed level with a pressure drop of around 0.5
MPa across the core. During soaking time, the slight pressure change of the core was observed which
might result from the dissolution of CO2 into oil phase. To investigate the effects of soaking time, three
different durations of soaking time, 10, 3, and 1 h, were implemented in the study. Eight series of cyclic
coresfloods, 35 runs in total were conducted, 32 runs carried out used pure CO2 as injection gas (runs 1
through 32) while runs 33 through 35 injecting N2 after CO2 injection as chasing gas. Experimental
conditions for this study are concluded in Table 5 and oil displacement results are presented in Table 6
and Figures 3 through 11.
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Figure 3RF comparison between Test 5 with an injection rate of 720cc/h and Test 6 with an injection rate of 480 cc/h.
The total recovery factor of the first three cycles of Tests 1 through 8 achieved in this study ranged
from 17.33% OOIP for Test 7 to as high as 29.52% OOIP for Test 4 and was observed to be sensitive to
the operation conditions, such as CO2 injection rate, gas slug size, maximum operation pressure, and
soaking time. The CO2 huff-n-puff technique is viable to recover the oil in low-pressure light oil reservoirs
with closed outer boundary.
4.2. Effects of the CO2 injection rate
The injection rate is one of the important operation parameters for CO2 huff-n-puff field applications. In
field operations of CO2 huff-n-puff process, CO2 is usually recommended to be injected at the highest rate
that the formations can hold, helping the gas phase penetrate as far into the rock and contact as much oil
as it can (Karim et al., 1992, Liu et al., 2005). In this study, to address the effects of the injection rate on
light-oil CO2 huff-n-puff process, two analogous five-cycle operations, test 5 (runs 20 through 24) and test
6 (runs 25 through 29), were performed under the same operation conditions except using two different
injection rates, 480 cc/h for test 5 and 720cc/h for teat 6. The test results were concluded in Table 6 and
also compared in Figure 3. The bar charts in Figure 3 show that the CO2 injection rate of 480cc/h, when
compared to the injection rate of 720 cc/h, is able to generate more favorable performance either for one
single cycle or one complete test. The improvement of the performance for the first two cycles is more
noticeable than other cycles. It seems that a smaller CO2 injection rate, such as 480 vs. 720cc/h, may lead
to a more successful CO2 cyclic operation. This trend is contrary to the observations seen in another
low-permeability corefloods (Wang et al, 2013) with the same boundary conditions as this study. In the
low-permeability corefloods, two CO2 injection rates of 60 and 140cc/hr were examined and it was found
that the injection rate of 140cc/h produced some performance improvement. On the basis of the
combination of the observations in those two coreflood, the optimal CO2 injection rate for a CO2
huff-n-puff application with a closed outer boundary should lie between 140- to 480cc/hr. Further
corefloods using intermediate injection rates are needed to identify its optimal vale. Neither a large
injection rate, such as 720cc/hr, nor a small one, such as 60cc/h can benefit the cyclic CO2 injection
processes. This observation is similar to that presented by Karim et al. (1992). In their study, the
injection rates of 60, 100, 140, 160, and 200 cc/h in first- and second-cycle operations of cyclic CO2
injection process were conducted using a watered-out conventional core. They observed that the
intermediate injection rate of 140 cc/hr was the optimal injection rate to maximize the overall process
performance. The observation differences between this study and Karim et al. may mainly lie in the
differences in simulated reservoir boundaries.
10
SPE-169235-MS
SPE-169235-MS
11
12
SPE-169235-MS
SPE-169235-MS
13
Based on the test results in this study, it is suggested that using different pressure depletion rates
may affect the process response positively or negatively, but the resulted effects were unmeasurable.
4.7. Effects of soaking time
Soaking time is a major consideration when designing a CO2 huff-n-puff process. To investigate
its effects on the process response and figure out
the optimal soaking period of the cyclic CO2 injections in low-pressure light oil reservoirs with
closed outer boundary, Tests 2 and 3 were conducted under similar conditions with an exception
of allowing different soaking periods. Long soaking periods were used in the successive cycles of
Figure 10 The performance comparison between Run 5 with 10 h
Test 2 (10-h soak time for the first cycle, Run 5, vs.
soaking time and Run 10 with 1 h soaking
3-h soaking time for the remaining four cycles,
Runs 6 through 9.) to have the core pressure stabilized, while a short soaking time of 1 hour was used
in each cycle of Test 3, Runs 10 through 14.
The results of those two Tests (listed in Table 6)
indicated that, for the first cycle, the oil recovery was
significantly increased by 15.5 % when the soaking
time was extended from 1 hour for Run 10 with a
recovery factor of 13.78% OOIP to 10 hours for Run
5 with a recovery factor of 15.91% OOIP. However, if
compared to Run 5 in terms of the average oil production rate, as plotted in Figure 10, the performance
of Run 10 was much favorable than that of Run 5. Run
10 achieved an average oil production rate of
Figure 11The performance comparison between Run 6 with 3 h
14.14108 BOPD, nearly as twice as that of Run 5,
soaking time and Run 11 with 1 h soaking
7.9108BOPD. It suggested that an over-extended
soaking time may greatly reduce the average oil production rate of the cycle operations.
For the second-cycle operations, as plotted in Figure 11, Run 6, allowing 3 hours soaking, exhibited
the slight improvement in oil recovery, 7.49% OOIP vs. 7.06% OOIP for Run 11, using 1 hour soaking,
but the measurable decrease in the average oil production rate, 7.1108 vs. 8.75108 BOPD for Run
11. The same observations can be obtained for the third-cycle operations, Runs 7 vs. 12.
It is indicated that a long soaking period, such as 10 hours in this study, helped a lot to improve the oil
recovery in the first cycle but simultaneously significantly decreased the average oil production rate of the
process. However, for the second- and third-cycle injections, allowing 3 hours vs. 1 hour to shut in did not show
a noticeable improvement in oil recovery while resulted in unfavorable average oil production rate. Different
from the observations of Wang et al. (2013), for low-pressure light oil CO2 huff-n-puff injections, the first cycle
rather than the second and third cycles was more sensitive to a long soaking time.
5 Conclusions
Based on the results of this study, some conclusions can be summarized as follows:
1. The CO2 huff-n-puff technique is viable to enhace oil recovery in low-pressure tight oil reservoirs
with a closed outer boundary.
14
SPE-169235-MS
2. The economically optimum huff-n-puff gas injection consists of three cycles with a potential
recovery factor of as high as 29.52% OOIP.
3. For the first cycle, a small CO2 slug size showed an attractive result. 0.1 PV CO2 plus a proper
amount of N2 as the chasing gas to build up the reservoir pressure seems to be the best injection
strategy in terms of the recovery factor and CO2 efficiency. Using more CO2 sequential cycles is
more favorable than than using large CO2 slug sizes.
4. The injection of N2 after a CO2 slug can dramatically reduce the usage of CO2. The performance
strongly depends on the maximum pressure built up during the gas injection period. It is
recommended that the injection pressure of CO2 huff-n-puff is better to be built up to as high as
rock permits.
5. High injection rates of CO2 is unfavorable for the oil production.
6. A soaking time is required in cyclic CO2 injection process with closed boundary to achieve
favorable recovery efficiency while a long soaking time may greatly decrease the average oil
production rate of a cycle. In this study, it was observed that the first cycle rather than two cycles
following it was more sensitive to a long soaking time.
7. The influence of pressure depletion rates were marginally to the performance of CO2 huff-n-puff.
Acknowledgements
The authors would like to acknowledge the permission for the pubilication of this paper from Yanchang
Petroleum (Group), China.
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