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ADX Report for Untitled Experiment

Today's date:
Experiment creation date:

01JAN1993
01JAN1993

Design Details
Design Details
Design Type
Number of factors
Number of runs
Resolution

Two-level
4
16
Full

Factors and Responses


Factor
C
M
T
P

Label
CONCENTRACION %
MEZCLADOR
TEMPERATURA C
PRESION

Low
30
M1
111
12

Center
45
0
116
13.25

High
Response
60 Y1
M2
121
14.5

Confounding Rules
No confounding rules

Design Points
Coded Design
Run
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16

Coded Factor Values


C
M
T
-1
-1
-1
1
-1
-1
-1
1
-1
1
1
-1
-1
-1
1
1
-1
1
-1
1
1
1
1
1
-1
-1
-1
1
-1
-1
-1
1
-1
1
1
-1
-1
-1
1
1
-1
1
-1
1
1
1
1
1

Response Values
P
-1
-1
-1
-1
-1
-1
-1
-1
1
1
1
1
1
1
1
1

Y1
71
65
60
65
90
95
86
96
85
88
68
80
83
85
75
70

Uncoded Design
Run
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16

C
30
60
30
60
30
60
30
60
30
60
30
60
30
60
30
60

Uncoded Factor Values


M
T
M1
111
M1
111
M2
111
M2
111
M1
121
M1
121
M2
121
M2
121
M1
111
M1
111
M2
111
M2
111
M1
121
M1
121
M2
121
M2
121

Response Values
P
12
12
12
12
12
12
12
12
14.5
14.5
14.5
14.5
14.5
14.5
14.5
14.5

Y1
71
65
60
65
90
95
86
96
85
88
68
80
83
85
75
70

Fit Details
Fit for Y1
ANOVA for Y1
Source DF
SS
C
1
42.25
M
1 240.25
T
1 600.25
P
1
2.25
C*M
1
20.25
C*T
1
0.25
C*P
1
0.25
M*T
1
6.25
M*P
1
72.25
T*P
1 812.25

Model
Error

10
5

Total

15 1919.75

Master Model
MS
F
42.25 1.713996
240.25 9.74645
600.25 24.35091
2.25 0.091278
20.25 0.821501
0.25 0.010142
0.25 0.010142
6.25 0.25355
72.25 2.931034
812.25 32.95132

Predictive Model
Pr > F DF
SS
MS
F
0.247401 1
42.25 42.25 1.713996
0.026195 1 240.25 240.25 9.74645
0.004342 1 600.25 600.25 24.35091
0.774722 1
2.25
2.25 0.091278
0.406299 1
20.25 20.25 0.821501
0.923696 1
0.25
0.25 0.010142
0.923696 1
0.25
0.25 0.010142
0.635981 1
6.25
6.25 0.25355
0.147571 1
72.25 72.25 2.931034
0.002248 1 812.25 812.25 32.95132

1796.5 179.65 7.288032 0.020333 10


123.25 24.65
5

Pr > F
0.247401
0.026195
0.004342
0.774722
0.406299
0.923696
0.923696
0.635981
0.147571
0.002248

1796.5 179.65 7.288032 0.020333


123.25 24.65

15 1919.75

Fit Statistics for Y1


Master Model

Predictive Model

RMSE
R-square
Adjusted R-square
Coefficient of Variation

4.964877
93.58%
80.74%
6.294614

4.964877
93.58%
80.74%
6.294614

Alias Structure for Y1


Master Model
No effects aliased.

Predictive Model
No effects aliased.

Predictive Model for Y1


Coded Levels(-1,1)
Y1 = 78.875 + 1.625*C - 3.875*M + 6.125*T + 0.375*P + 1.125*C*M
- 0.125*C*T - 0.125*C*P + 0.625*M*T - 2.125*M*P - 7.125*T*P
Uncoded Levels
Y1 = -1836.16 + 0.465*C - 1.55*(M='M1') + 16.53*T + 131.14*P
- 0.15*C*(M='M1') - 0.001667*C*T - 0.006667*C*P - 0.25*T*(M='M1')
+ 3.4*P*(M='M1') - 1.14*T*P

Effects for Y1
Term Estimate
C
3.25
M
-7.75
T
12.25
P
0.75
C*M
2.25
C*T
-0.25
C*P
-0.25
M*T
1.25
M*P
-4.25
T*P
-14.25

Master Model
Std Err
t
2.482438 1.309197
2.482438 -3.12193
2.482438 4.934664
2.482438 0.302122
2.482438 0.906367
2.482438 -0.10071
2.482438 -0.10071
2.482438 0.503537
2.482438 -1.71203
2.482438 -5.74032

Pr > |t| Estimate


0.247401
3.25
0.026195
-7.75
0.004342
12.25
0.774722
0.75
0.406299
2.25
0.923696
-0.25
0.923696
-0.25
0.635981
1.25
0.147571
-4.25
0.002248
-14.25

Predictive Model
Std Err
t
2.482438 1.309197
2.482438 -3.12193
2.482438 4.934664
2.482438 0.302122
2.482438 0.906367
2.482438 -0.10071
2.482438 -0.10071
2.482438 0.503537
2.482438 -1.71203
2.482438 -5.74032

Pr > |t|
0.247401
0.026195
0.004342
0.774722
0.406299
0.923696
0.923696
0.635981
0.147571
0.002248

Optimization Details
Desirability
Y1
D(Y1)
D(Y1)
D(Y1)
Power
Power

=
=
=
=
=

0 when Y1
0.5 when Y1
1 when Y1
1 for lower half
1 for upper half

<
=
>

70
82.5
95

Prediction Profile Settings


Factor
C
M
T
P

Label
CONCENTRACION %
MEZCLADOR
TEMPERATURA C
PRESION

Optimal Setting

Response
Y1
45 Desirability

Estimated Value
82.75
51.00%

M1
116
13.25

ADX Report for Untitled Experiment


Today's date:
Experiment creation date:

01JAN1993
01JAN1993

Design Details
Design Details
Design Type
Number of factors
Number of runs
Resolution

Two-level
4
16
Full

Factors and Responses


Factor
K

Label
CATALIZADOR LBM

Low
10

Center
12.5

High
Response
15 Y1

T
P
C

TEMPERATURA C
PRESION PSI
CONCENTRACION %

220
50
10

230
65
11

240
80
12

Confounding Rules
No confounding rules

Design Points
Coded Design
Run
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16

Coded Factor Values


K
T
P
-1
-1
-1
1
-1
-1
-1
1
-1
1
1
-1
-1
-1
1
1
-1
1
-1
1
1
1
1
1
-1
-1
-1
1
-1
-1
-1
1
-1
1
1
-1
-1
-1
1
1
-1
1
-1
1
1
1
1
1

Response Values
C
-1
-1
-1
-1
-1
-1
-1
-1
1
1
1
1
1
1
1
1

Y1
71
61
90
82
68
61
87
80
61
50
89
83
59
51
85
78

Uncoded Design
Run
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16

Uncoded Factor Values


K
T
P
10
220
50
15
220
50
10
240
50
15
240
50
10
220
80
15
220
80
10
240
80
15
240
80
10
220
50
15
220
50
10
240
50
15
240
50
10
220
80
15
220
80
10
240
80
15
240
80

Response Values
C
10
10
10
10
10
10
10
10
12
12
12
12
12
12
12
12

Y1
71
61
90
82
68
61
87
80
61
50
89
83
59
51
85
78

Fit Details
Fit for Y1
Check Assumptions Analysis for Y1
Response Transformation
Optimal transformation from Box-Cox plot
Transformation recommended by ADX
Transformation applied for analysis
Response scaling shift
Outlier Observations
Run numbers deleted from analysis
Influential Observations
Run numbers deleted from analysis

Y1**2
Y1
Y1
0
None
None

ANOVA for Y1
Source DF SS
K
1 256
T
1 2304
P
1 20.25
C
1 121
K*T
1
4

Master Model
MS
F
Pr > F DF
256 213.3333
0.0001 1
2304
1920
0.0001 1
20.25
16.875 0.009283 1
121 100.8333 0.000168 1
4 3.333333 0.127464

K*P

2.25

2.25

K*C

T*P
T*C
P*C

1
1
1

6.25
81
0.25

Predictive Model
SS
MS
F
Pr > F
256
256 136.5333
0.0001
2304 2304
1228.8
0.0001
20.25 20.25
10.8 0.008201
121
121 64.53333
0.0001

1.875 0.229205
0

6.25 5.208333 0.071344


81
67.5 0.000435
0.25 0.208333 0.667219

Model
Error

10 2795 279.5 232.9167


5
6
1.2

Total

15 2801

0.0001

43.2

0.0001

5 2782.25 556.45 296.7733


10
18.75 1.875

0.0001

15

81

81

2801

Fit Statistics for Y1


RMSE
R-square
Adjusted R-square
Coefficient of Variation

Master Model
1.095445
99.79%
99.36%
1.516187

Predictive Model
1.369306
99.33%
99.00%
1.895234

Alias Structure for Y1


Master Model

Predictive Model

No effects aliased.

No effects aliased.

Predictive Model for Y1


Coded Levels(-1,1)
Y1 = 72.25 - 4*K + 12*T - 1.125*P - 2.75*C + 2.25*T*C
Uncoded Levels
Y1 = 420.625 - 1.6*K - 1.275*T - 0.075*P - 54.5*C + 0.225*T*C

Effects for Y1
Master Model
Predictive Model
Term Estimate Std Err
t
Pr > |t| Estimate Std Err
t
K
-8 0.547723 -14.6059
0.0001
-8 0.684653 -11.6847
T
24 0.547723 43.8178
0.0001
24 0.684653 35.05424
P
-2.25 0.547723 -4.10792 0.009283
-2.25 0.684653 -3.28634
C
-5.5 0.547723 -10.0416 0.000168
-5.5 0.684653 -8.03326
K*T
1 0.547723 1.825742 0.127464
K*P
K*C
T*P
T*C
P*C

Pr > |t|
0.0001
0.0001
0.008201
0.0001

0.75 0.547723 1.369306 0.229205


0 0.547723

-1.25 0.547723 -2.28218 0.071344


4.5 0.547723 8.215838 0.000435
-0.25 0.547723 -0.45644 0.667219

4.5 0.684653 6.572671

0.0001

Optimization Details
Desirability
Y1
D(Y1)
D(Y1)
D(Y1)
Power
Power

=
=
=
=
=

0 when Y1
0.5 when Y1
1 when Y1
1 for lower half
1 for upper half

<
=
>

55
72.5
90

Prediction Profile Settings


Factor
K
T
P
C

Label
CATALIZADOR LBM
TEMPERATURA C
PRESION PSI
CONCENTRACION %

Optimal Setting

Response
Y1
12.5 Desirabil
230
65
11

Estimated Value
72.25

EL PRIMERO

ADX Report for Untitled Experiment


Today's date:
Experiment creation date:

01JAN1994
01JAN1994

Design Details
Design Details
Design Type
Number of factors
Number of runs
Resolution

Two-level
3
8
Full

Factors and Responses

Factor
T
C
K

Label
TEMPERATURA C
CONCENTRACION %
CATALIZADOR

Low
160
20
A

Center
170
30
0

High
Response
180 Y1
40
B

Confounding Rules
No confounding rules

Design Points
Coded Design
Run
Number
1
2
3
4
5
6
7
8

Coded Factor Values


T
C
-1
-1
1
-1
-1
1
1
1
-1
-1
1
-1
-1
1
1
1

Response Values
K
-1
-1
-1
-1
1
1
1
1

Y1
60
72
54
68
52
83
45
80

Uncoded Design
Run
Number
1
2
3
4
5
6
7
8

Uncoded Factor Values


T
C
160
20
180
20
160
40
180
40
160
20
180
20
160
40
180
40

Response Values
K
A
A
A
A
B
B
B
B

Y1
60
72
54
68
52
83
45
80

Fit Details
Fit for Y1
Check Assumptions Analysis for Y1
Response Transformation
Optimal transformation from Box-Cox plot
Transformation recommended by ADX
Transformation applied for analysis
Response scaling shift
Outlier Observations

Y1**2
Y1**2
Y1
0

Outlier statistic
Outlier criterion
Run numbers deleted from analysis
Influential Observations
Run numbers deleted from analysis

Poutlier
0.05
None
None

ANOVA for Y1
Source DF
T
1
C
1
K
1
T*C
1
T*K
1
C*K
1

Master Model
SS
MS
F
1058 1058 2116
50
50 100
4.5
4.5
9
4.5
4.5
9
200
200 400
0
0
0

Model
Error

6
1

1317 219.5
0.5
0.5

Total

7 1317.5

Pr > F DF
0.013837 1
0.063451
0.204833 1
0.204833
0.031805 1
1

439 0.036518

SS
1058

Predictive Model
MS
F
Pr > F
1058 76.94545 0.000931

4.5

4.5 0.327273 0.597885

200

200 14.54545 0.018878

3 1262.5 420.8333 30.60606 0.003222


4
55
13.75
7 1317.5

Fit Statistics for Y1


Master Model
0.707107
99.96%
99.73%
1.100555

RMSE
R-square
Adjusted R-square
Coefficient of Variation

Predictive Model
3.708099
95.83%
92.69%
5.771361

Alias Structure for Y1


Master Model
No effects aliased.

Predictive Model
No effects aliased.

Predictive Model for Y1


Coded Levels(-1,1)
Y1
= 64.25 + 11.5*T + 0.75*K + 5*T*K
Uncoded Levels
Y1
= -215.5 + 1.65*T + 168.5*(K='A') - T*(K='A')

Effects for Y1
Term

Master Model
Estimate Std Err t

Pr > |t|

Estimate

Predictive Model
Std Err
t

Pr > |t|

T
C
K
T*C
T*K
C*K

23
-5
1.5
1.5
10
0

0.5 46
0.5 -10
0.5
3
0.5
3
0.5 20
0.5
0

0.013837
0.063451
0.204833
0.204833
0.031805
1

23

2.622022

8.771856

0.000931

1.5

2.622022

0.572078

0.597885

10

2.622022

3.81385

0.018878

Optimization Details
Desirability
D(Y1)
D(Y1)
D(Y1)
Power
Power

Y1
0 when Y1
0.5 when Y1
1 when Y1
1 for lower half
1 for upper half

=
=
=
=
=

<
=
>

45
62.5
80

Prediction Profile Settings


Factor
T
C
K

Label

Optimal Setting

TEMPERATURA C
CONCENTRACION %
CATALIZADOR

Response
Y1
170 Desirability

Estimated Value
63.5
52.86%

30
A

Numerical Optimization Results


TEMPERATURA C

CONCENTRACION %
180
180
180
180
180
175
175
175
175
175
180
180
180
180
180
175
175
175
175
175
170

CATALIZADOR
20 B
25 B
30 B
35 B
40 B
20 B
25 B
30 B
35 B
40 B
20 A
25 A
30 A
35 A
40 A
20 A
25 A
30 A
35 A
40 A
20 B

Y1
81.5
81.5
81.5
81.5
81.5
73.25
73.25
73.25
73.25
73.25
70
70
70
70
70
66.75
66.75
66.75
66.75
66.75
65

170
170
170
170

25 B
30 B
35 B
40 B

65
65
65
65

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