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To cite this article: S. Krishnan, D. V. Kulkarni & A. De (2016) Multipass pulsed current gas
metal arc welding of P91 steel, Science and Technology of Welding and Joining, 21:3, 171-177,
DOI: 10.1179/1362171815Y.0000000080
Article views: 12
Elements (wt-%) C Cr Mo V Ni Si Mn Al Nb N
Base metal (P91 steel) 0.10 9.01 0.89 0.21 0.24 0.21 0.41 0.02 0.08 0.05
Electrode (ER90S-B9) 0.11 8.93 0.94 0.20 0.66 0.23 0.55 ... 0.06 0.03
microstructure and mechanical properties.30,31 A recent (Graphtec made, model no. GL 900-4) with simultaneous
study on single-pass GMAW-P of P91 steel showed a sampling rate of 0.1 MHz is used to monitor the current and
fair improvement of the weld chemistry and mechanical the voltage transients. The corresponding time-averaged
properties over the similar joints prepared using con- current IAV and voltage VAV are estimated as
ventional GMAW.32
A detailed investigation on multipass GMAW-P of I P tP I B tB
I AV 1
12 mm thick P91 steel is undertaken in the present work. tP tB
The effects of welding current, speed and groove geo- V P tP V B tB
metry on the bead profile, weld chemistry and oxygen V AV 2
tP tB
content, weld toughness and tensile strengths and
susceptibility to the formation of delta ferrite and non- where IP, IB, VP, VB, tP and tB refer respectively to the peak
metallic inclusions are examined. The multipass weld pulse and base current, peak and base voltage and the cor-
cross-sections are examined critically for adequacy of responding time durations in a currentvoltage cycle. For a
the side-wall and inter-bead fusions. The hardness dis- current setting, the variability in the time-averaged current
tribution is tested across the weld and HAZ regions both and voltage are estimated over 20 currentvoltage pulses.
in as-welded and after PWHT. Table 2 documents the measured values of the pulse
parameters and the estimated values of the time-averaged
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current and the heat input per unit length. The time-aver-
Experimental investigation aged value of voltage remains around 26 V for all the three
Table 1 presents the composition of workpiece and electrode current settings.
materials. The base material conforms to 12 mm thick The welded coupons were subjected to PWHT for
modified 9Cr1Mo (P91) steel with impact toughness, ulti- stress relieving at 760108C for 4 h. The transverse
mate tensile strength and yield strength of respectively 220 J, weld cross-sections were examined after polishing and
670 MPa and 550 MPa at room temperature. Figure 1 etching with Villellas reagent (1 g picric acid, 5 mL
schematically shows the joint geometry. Multipass bead-in- hydrochloric acid, and 100 mL methanol). The bead
groove welds are prepared in flat (1G) position with microstructures are examined under a scanning electron
Ar+2%CO2 shielding gas using a backhand technique at microscope (SEM) in as-welded condition and after
multiple combinations of current, speed and groove angle PWHT. The microhardness distribution was measured
following a three-level full factorial design with three in as-welded condition and after PWHT at various lo-
repetitions at each welding condition. Three levels of weld- cations as shown in Fig. 2. The tensile strength was
ing speed and current setting are chosen as follows: 310, 320, evaluated using all-weld sub-size specimens as per
and 330 mm min21 and 255, 263, 270 A respectively. Three ASTM E8:2013.33 The weld toughness was evaluated
different groove angles of 45u, 60u and 75u are considered as using sub-size specimens as per ASTM A370:2014.34
shown in Fig. 1. A microprocessor controlled synergic A spectrometer based weld bead chemical analysis was
GMAW-P power source is used to prepare the weld carried out as per ASTM E415:2014.35 The oxygen
samples. A four-channel transient recorder content in the weld was studied by wet analysis following
ASTM E1019:2011.36 The weld inclusion level was
examined using energy dispersive spectroscopy analysis.
Table 2 Details of pulse parameters and corresponding heat input per unit length (superscripts a, b, and c refer to estimated
heat input at welding speeds of 310, 320 and 330 mm min21)
255 343 (10) 91 (5) 2.24 (1) 3.98 (1) 182 (6) 160 0.91a, 0.88b, 0.85c
263 351 (15) 104 (3) 2.25 (1) 3.49 (1) 199 (7) 175 1.01a, 0.99b, 0.96c
270 357 (8) 114 (3) 2.27 (1) 3.38 (1) 212 (5) 178 1.10a, 1.07b, 1.04c
3 Macrographs of weld transverse sections at welding speed of 320 mm min21 and current setting of 263 A at groove angles
of a 458, b 608, c 758 and d 608 showing typical LF defect
Table 3 Weld metal compositions (in wt-%) in GMAW-P to examine the consistency of the measured values across
the weld bead. In general, the toughness along location 1
Groove angle
are found to be slightly higher that is attributed to the
effective tempering of this region during subsequent
Elements 458 608 758
weld passes and resulting finer microstructure. Figure 6b
Mn 0.440.49 0.430.50 0.460.51 shows the effect of heat input per unit length on the
Si 0.160.21 0.170.22 0.180.21 average weld bead toughness (at +20uC) for different
Cr 8.709.00 8.759.10 8.809.08 welding conditions. The weld bead toughness is found to
Ni 0.350.40 0.350.40 0.380.40 reduce with an increase in the heat input per unit length
Mo 0.850.96 0.830.98 0.890.96 for the 75u and 60u groove angles. The measured
Nb 0.0600.065 0.0580.065 0.0600.065
S 0.0020.004 0.0020.004 0.0020.004
toughness values for the welds with the 45u groove angle
O2 0.0490.053 0.0490.052 0.0490.053 are not plotted as the same are found to be scattered
C 0.1150.120 0.1160.120 0.1150.120 within a range of 42 to 55 J that is attributed to the large
V 0.190.20 0.190.20 0.180.20 number of defects in these welds. The decrease in the
N 0.0500.051 0.0500.051 0.0490.051 weld toughness with an increase in the heat input per
unit length is attributed primarily to the reduced cooling
rate and resulting coarser grain structure. Further, the
distribution across the P91 welds before and after PWHT. weld bead toughness is found to increase with an
Figure 5 shows the FZ microhardness to be higher increase in the groove angle for a given heat input per
compared to that in base material and HAZ regions in unit length that is attributed to the decrease in weld
as-welded condition. The FZ depicts a cast structure in the defects at higher groove angles. The weld bead tough-
as-welded condition leading to higher hardness in com- ness is also affected by the size and density of the micro-
parison to the same in the normalised and tempered inclusions in the bead microstructure. Figure 7 shows
structure of the base material.10 The microhardness the distribution of spherical micro-inclusions with Al, Si,
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becomes nearly uniform after PWHT except a softer region Mn and Fe respectively around 5.96%, 5.77%, 7.86%
in ICHAZ due to partial transformation of austenite and 79.59% as obtained from an SEMenergy dispersive
structure and subsequent tempering during PWHT.1 The spectroscopy analysis. An inclusion rating analysis as
overall width of the HAZ remains between 3.0 and 3.5 mm per ASTM E-45:201338 has shown that the size of these
in contrast to 4.5 to 5.0 mm as observed in GTAW and inclusions is lesser than 2 mm that is significantly lower
SMAW of P91 steels.14 The reduction in HAZ width in than those obtained in FCAW11 and single-pass
GMAW-P can be considered significantly beneficial GMAW-P.32 The smaller size of inclusions in multipass
towards reducing the susceptibility to type IV cracking in GMAW-P of P91 welds is attributed to the remelting of
welds of P91 steel.1,13 the underneath weld beads during multiple weld passes
The weld bead toughness for each sample weld is and resulting disintegration of the coarser micro-in-
evaluated at three different locations as shown in Fig. 6a clusions and formation of numerous finer particles.
4 a Base metal, b FZ in as-welded condition, and c FZ, d CGHAZ, e FGHAZ, and f ICHAZ microstructures after PWHT at 7608C
for 4 h for sample welds at current setting of 263 A, welding speed of 320 mm min21 and groove angle of 758
5 Microhardness variation across weld bead at current setting of 263 A, welding speed of 320 mm min21 and groove angle of
758 in as-welded condition and after PWHT
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6 a Notch locations for weld toughness measurement, b measured values of weld toughness as function of heat input per unit
length and at two different groove angles of 608 and 758
Table 4 Compositions (average) and properties of P91 weld for current of 255 A and welding speeds of 310, 320 and
330 mm min21 with 758 groove angle in conventional GMAW
Elements Mn Si Cr Ni Mo Nb O2 C V N Al
wt-% 0.38 0.19 8.68 0.30 0.85 0.05 0.063 0.12 0.19 0.04 0.02
HAZ width/mm 4.204.95 Toughness/J 2642 UTS/MPa 675692
Figure 8 presents the all-weld tensile strength of the flux related problems similar to SMAW, FCAW and
sample welds. The measured ultimate tensile strength SAW processes. A detailed investigation of the suit-
(UTS) indicates a similar trend as noticed in the weld ability of GMAW-P for the joining of P91 steels is
bead toughness in Fig. 6b. The measured values of therefore requisite and currently scarce in the literature.
UTS reduce with an increase in the heat input per unit The work presented here demonstrates a critical exam-
length for the welds made with the 60u and 75u groove ination of the effects of the key welding variables on the
angles. In contrast, the measured strengths for the welds final weld bead quality in multipass GMAW-P of 12 mm
produced with 45u groove angle exhibited a wide thick P91 steel. The welds are found to be fairly accep-
scatter in between 650 and 720 MPa that is attributed table based on the visual inspection of the bead profile,
to the inherent defects and were not plotted. The composition analysis, oxygen and inclusion levels, and
maximum all-weld UTS is obtained as 760 MPa the examination of microhardness distribution, micro-
with the 75u groove angle for a current setting of 255 A structure, mechanical strength and toughness. An
and welding speed of 330 mm s21 that con-forms to appropriate selection of the heat input per unit length
a low heat input per unit length of 0.85 kJ and groove geometry is found to be critical. In par-
mm21. An increase in all-weld UTS at lower heat input ticular, the groove angle should be sufficiently large to
per unit length can be attributed to the get a defect free weld. An average heat input per unit
smaller dendrite sizes and lesser interdendritic spacing length of 0.85 kJ mm21 with a groove angle of 75u
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