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www.springerlink.com/content/1738-494x(Print)/1976-3824(Online)
DOI 10.1007/s12206-017-0234-x
(Manuscript Received May 27, 2015; Revised March 15, 2016; Accepted October 26, 2016)
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Abstract
In the current scenario cladding process are used in many engineering industries to enhance the corrosion resistance surface and wear
resistance of the base material in chloride environment. Cladding of stainless steel results in formation of ferrite number content on clad-
ded surface, which deleterious the material properties. The present investigation address the effect of process parameters on ferrite num-
ber during austenitic stainless steel 317L cladding by Pulsed Metal inert gas (MIG) welding process. Ferrite number was measured by
using Fisher’s ferrite scope. Response surface methodology (RSM) based central composite rotatable design were approached to predict
and develop the mathematical model for process parameters such as welding current, welding speed and contact tip to work distance on
ferrite number. From the analysis of variance technique it is found that the developed mathematical model was significant. The devel-
oped mathematical model is useful to control and determine the ferrite number content in austenitic stainless steel cladding. The direct
and interaction effects of input process parameters are presented graphically.
Keywords: Ferrite number; Pulse cladding; Prediction; Response surface methodology; Stainless steel
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rial property. Hence it is very important to obtain the optimal Table 1. Chemical composition of base material and filler wire
number of ferrite number during cladding [13]. In this row (Weight percent).
Kannan and Murugan [14] predicted the ferrite number of Materials C Si Mn P S Cr Ni Cu Mo Fe
duplex stainless steel cladded metals by using response sur- Base
face methodology. 0.23 0.31 0.93 0.05 0.02 - - - - 98.46
material
The mathematical models were developed to predict the Filler
delta ferrite content during cladding of austenitic stainless 0.03 0.65 2.5 0.04 0.03 20 15 0.75 4 57
wire
steel and duplex stainless steel using response surface meth-
odology [15, 16]. Vasudevan et al. [17] used Bayesian neural Table 2. Process variables and experimental levels.
network to develop the mathematical for the prediction of
delta ferrite content in stainless steel weld. Process Levels
Symbols
parameters -1.682 -1 0 +1 +1.682
Rao et al. [18] studied the effect of process parameters on
bead geometry during pulsed gas metal arc welding using Welding
I 190 200 215 230 240
Taguchi method. Mathematic models were developed using current
multiple regression analysis and validated the adequacy. Fur- Welding
S 170 180 195 210 220
ther it was found that predicted models for the responses are speed
within reasonable accuracy. Contact tip to
N 17 18 20 21 22
Pal et al. [19] made a study on optimization of process pa- work distance
rameters for quality characteristic by using grey-based Ta-
guchi method. It was found that the process parameter has solid wire of diameter 1.2 mm was used as filler wire and low
more influence on quality characteristic by ANOVA. Re- carbon structural steel IS: 2062 of 20 mm thickness plate was
sponse surface methodology based central composite rotatable used as base material. The chemical composition of the base
design in design expert software technique is mostly used for material and filler wire are shown in Table 1.
developing the experimental design matrix. It is the simplest
method for developing a mathematical model and correlate
2.2 Experimental methods
relationship between process parameters and response. It is
useful to discuss the main effect and interaction effects [20- There are various methods to conduct the experiments such
22]. as Taguchi method [19], grey relational analysis, orthogonal
The above literatures clearly show that identifying and se- array, full factorial design [20], and artificial intelligence [17],
lecting the process parameters for the cladding process is chal- face centered composite design and central composite ro-
lenging one for many research works. However response sur- tatable design [11, 22]. Response surface methodology based
face methodology based central composite rotatable design central composite rotatable design technique was used to de-
technique was used by various researchers for developing sign the experimental matrix to perform the experiments. This
mathematical model and analysing the process parameters. design is generally used by maximum number of researchers
Hence the study related to prediction of ferrite number in for obtaining minimum number of experimental runs with
Pulsed MIG welding was not that much discussed. good accuracy and developing the second order polynomial
There was various attempts have been made to develop the regression equation [11, 15]. Based on the literature analysis,
mathematical model for prediction of ferrite number by using the three factors are considered for this present investigation
nickel and chromium alloy composition. It was found that such as welding current (I), welding speed (S) and contact tip
very few works was discussed about prediction of ferrite to work distance (N). Bead-on-plate type welding were per-
number based on process parameters. formed with changing the process parameters values and ex-
In this present investigation, the effects of process parame- amine the appearance of the bead process parameters levels
ters on ferrite number in Pulsed MIG welding during 317L are selected for this investigation, their upper limits and lower
solid stainless steel wire cladded on structural steel plate IS: limits of each process parameters are fixed respectively. The
2062 was studied by following approach. upper limits and lower limits of a process parameters was
By conducting the weld cladding of 317L austenitic stain- coded as +1.682 and -1.682 respectively, the coded values of
less steel onto structural steel IS: 2062. Preparing the speci- the intermediate levels being calculated from the Eq. (1)
men as per metallurgical procedure and ferrite number was shown in Table 2 [9].
measured by using Fishers ferrite scope. By developing the
quadratic polynomial equation and analysing their effects.
(1)
2. Experimentation
2.1 Experimental materials
where Xi is the required coded value of a variable X, X is any
In this investigation austenitic stainless steel AISI 317L of value of the variable from X min to X max, X min is the lower
R. Prabhu and T. Alwarsamy / Journal of Mechanical Science and Technology 31 (3) (2017) 1341~1347 1343
Table 4. Calculated β coefficients values for ferrite number model. Table 5. ANOVA table for ferrite number.
Eq. (4).
S : The welding speed mm/min and 3.1 Validation of developed mathematical model
N : The contact tip to work distance mm.
From the above mathematical model, the effects of process
Relationship between the response and the process variable parameters on ferrite number were examined. The Eq. (4) it is
are unknown. In order to study the main effect and interaction clear that the positive values of the polynomial coefficients
of the process parameters a second order polynomial response increases and negative values decreases the response. Analysis
surface can be fitted into the following Eq. (3) [21, 22]. of variance technique was further used to validate the ade-
quacy of the developed mathematical model. The F-value of
k k
y = b 0 + å b i xi + å b ii xi2 + åå b ij xi x j + e (3) 119.28 implies the model is significant at 95 % of confident
i =1 i =1 i j level. To check the goodness of the fitted model the coeffi-
i≠j cient of determination R2 and adjusted coefficient of determi-
nation R2 are calculated. The value of calculated R2 should lie
where βo is the free term of the regression equation. on 0-1 accordingly R2 is 0.99 it is very closer to 1 indicated
The coefficients of β1, β2 and β3 are linear terms. that the developed model is good. Adjusted coefficient of
The coefficients of β11, β22 and β33 are the quadratic terms. determination R2 is 0.98 which is high nearer to coefficient of
The coefficients of β12, β13 and β23 are the interaction terms. determination R2 0.9908 agrees that model is adequate it was
shown in Table 5. The coefficient of variation and adequate
precision ratio are found 2.65 and 33.986, respectively. The
2.6 Calculating the coefficients of the models
coefficient of variation is less than 5 and adequate precision
The values of the β coefficients in the second order poly- ratio is greater than 4.
nomial equation are calculated by using design expert soft-
ware and coefficients values are tabulated in Table 4. 3.2 Scatter diagram
Contact tip
Welding Welding Predicated Measured
No to work Error %
current speed FN FN
distance
1 212.55 202.7 19.46 0.53791 0.55138 2.50413
2 207.89 198.02 20.15 0.54783 0.56771 3.62886
3 209.83 201.08 18.91 0.53662 0.53210 0.84231
4 217.53 205.16 18.93 0.53467 0.54961 2.79424
4. Conformation test
The conformation test was conducted to evaluate the devel-
oped polynomial equation Eq. (4). The three conformation test
run were conducted with different combination of process
parameters predicted from software. The ferrite number was
measured and differences in predicted and measured values
are calculated by using error calculation equation Eq. (5). The
values are tabulated in Table 6.
Fig. 7. Effect of contact tip to work distance on Ferrite number.
Measured value - Predicted value
% Error = * 100 . (5)
Predicted value 5.2 Effect of welding speed on ferrite number
6. Conclusion
·A five-level, three factor design matrix based on central
composite rotatable design approach was used for the
development of mathematical models to predict the fer-
rite number for cladding of austenitic stainless steel 317L
deposited using pulsed MIG welding process.
·The predicted values using developed model as well as
experimental values are closer to each other.
Fig. 8. 3D Surface plot showing an interaction effect of welding cur-
·Welding current and welding speed are the most signifi-
rent and welding speed on ferrite number.
cant factor in prediction of ferrite number than with the
contact tip to work distance.
·The significant factors are identified by ANOVA. The
model values are adequate with 95 % of confidence level.
·Ferrite number decreases constantly with the increase in
welding speed due to the reduced deposition of filler ma-
terial over the base metal. However, the ferrite number
increases with the increase in welding current.
Nomenclature------------------------------------------------------------------------
I : Welding current
Fig. 9. 3D Surface plot showing an interaction effects of Welding S : Welding speed
speed and contact tip to work distance on Ferrite number. N : Contact tip to work distance
FN : Ferrite number
speed on ferrite number are shown in Fig. 8. It is clear that at SS : Sum of squares
lower level of the welding current with lower level of welding DoF : Degree of freedom
speed the ferrite number was considerably at mid value of the
graph. But when the welding current increases there are
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