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LECTURE 5: SEQUENCING OF
AZEOTROPIC DISTILLATION COLUMNS
Daniel R. Lewin
Department of Chemical Engineering
Technion, Haifa, Israel
Ref: Seider, Seader and Lewin (1999), Section 5.6
Assess Primitive
Problem
SECTION B
Detailed Design,
Equipment sizing, Cap.
Cost Estimation,
Profitability Analysis,
Optimization
0.2 TBA
0.65 DTBP
0.2 DTBP
0.15 H2O
0.2 TBA
0.2 DTBP
0.6 H2O
f f
j j
y P x f
j
V
j j j j
L
yP xP
1 1 1
s
yP xP
2 2 2
s
P x P x P x P (1 x )P
1 1
s
2 2
s
1 1
s
1 2
s
P (P P )x
2
s
1
s
2
s
At fixed temperature
1 1 1 1 2 2
1 1 1 1 2 2
Distillation still
As L 0:
Lx y dL Lx Ldx x dL dLdx , j 1, ,C 1
j j j j j j
dx
Rearranging: j
x y x (1 K {T, P, x, y })
dL / L
j j j j
dx j
x y
dt
j j
dh
n n 1
Substituting:
dx V D
x n
y x n
dh L L
n n D
n 1 n 1
Try toluene
as an
entrainer
M1
S1
S2
D2