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  • Comparing extractive distillation parameters

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    1) The document compares the performance of conventional distillation columns and extractive dividing wall columns (EDWC) for separating several binary mixtures. 2) EDWCs were able to achieve energy savings of 5-52% compared to conventional distillation with comparable or lower total annual costs for all mixtures studied. 3) Methylal-methanol separation saw the largest energy savings of 52% using an EDWC compared to conventional distillation.

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    1) The document compares the performance of conventional distillation columns and extractive dividing wall columns (EDWC) for separating several binary mixtures. 2) EDWCs were able to achieve energy savings of 5-52% compared to conventional distillation with comparable or lower total annual costs for all mixtures studied. 3) Methylal-methanol separation saw the largest energy savings of 52% using an EDWC compared to conventional distillation.

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    10 views5 pages

    Comparing extractive distillation parameters

    Uploaded by

    nobody666
    1) The document compares the performance of conventional distillation columns and extractive dividing wall columns (EDWC) for separating several binary mixtures. 2) EDWCs were able to achieve energy savings of 5-52% compared to conventional distillation with comparable or lower total annual costs for all mixtures studied. 3) Methylal-methanol separation saw the largest energy savings of 52% using an EDWC compared to conventional distillation.

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    of 5

    tabel ....

    extractive distillation konvensional dua kolom


    Campuran Entrainer
    jumlah tahap Jumlah energi(kW) TAC (1000 $/thn)
    Etanol-air Etylen Glycol 33 2007.82
    Etil Asetat-IPA 40 279 124
    jumlah tahap Jumlah energi(Gcal/h) TAC (1000 $/thn)
    Benzene-cyclohexane 34.3 6521.1

    Etanol-Air (Kiss 2012) Methylal-Methanol (Xia,2012)


    parameter CEDC EDWC CEDC EDWC
    N 33 20 64 64
    Q (KW) 2007.82 1819.52 1072.1 983.2
    Savings (%) 0 -9.38 0 -8.29
    TAC(1000$/year) ? ? 858.86 759.3
    Savings (%) - 0 -11.59
    VARIABEL TETAP
    LETAK
    umpan 13 13 41 35
    solvent 3 3 4 4
    side stream 7 5
    FLOW RATE kmol/h kg/h

    umpan 100 100 3000 3000


    solvent 190 190
    distilat 2576 2576
    REFLUX RATIO (asumsi) asumsi kolom 1 = 2 ; kolom 2 =0,5
    kolom 1 /dwc 0,3 0,2 1,2 1,295

    kolom 2/prefrac 1,15 0,27 0,595 0,118


    PRESSURE DROP 0,7 kpa 0,7 kpa
    TEKANAN 1 1
    liq vap ratio
    acetone-methanol (Wu, etanol-air (Tututiavila,2014)
    parameter 2013)
    CEDC EDWC CEDC EDWC
    N 83 70 36 21
    Q (KW) 18038.67 16284.6 1137.63 992.48
    Savings (%) 0 -9.72 0 -12.76
    TAC(1000$/year) 4252.96 4176.77 378.2 331.2
    Savings (%) 0 -1.79 0 -12.43
    extractive dividing-wall collumn
    jumlah tahap Jumlah energi(kW) TAC (1000 $/thn)
    20 1819,52(-9,38%)
    34 265(-5,02%) 111 (-10,48%)
    jumlah tahap Jumlah energi(Gcal/h) TAC (1000 $/thn)
    26,9(-21,57%) 6208,1(-4,8%)

    Benzene-cyclohexane acetone-methanol (Wu,


    Etil asetat-IPA (Zhang 2014) (Sun,2014) 2013)
    CEDC EDWC CEDC EDWC CEDC EDWC
    40 34 ? ? 83 70
    279 265 39890.9 31284.7 18038.67 16284.6
    0 -5.02 0 -21.57 0 -9.72
    124 111 6521.1 6208.1 4252.96 4176.77
    0 -10.48 0 -4.80 0 -1.79

    22 20 18 19 40 40
    5 5 8 8 25 25
    4 7 14
    kg/h kmol/h

    1000 1000 1000 1000 540 540


    1000 1000 2700 2700 1100 1100
    700,4 700,5 250 250

    2,37 2 4,2 3,8 3,32 3,32

    0,133 1,38 0,77 0,74 1,6 0,88


    0,0068 0,0068
    1 1 1 1 3 3
    0,67 0,67 0,68 0,68
    metanol-touluen-air
    (Yang,2018)
    CEDC EDWC
    122 60
    6552 3090
    0 -52.84
    1733 872
    0 -49.68
    etanol-air metanol-
    (Tututiavila,201 touluen-air
    4) (Yang,2018)
    CEDC EDWC CEDC EDWC
    36 21 122 60
    1137.6 992.48 6552 3090
    0 -12.76 0 -52.84
    378.2 331.2 1733 872
    0 -12.43 0 -49.68

    17 19
    11 11

    45,36 45,36
    69,6 69,6

    0,64 0,39

    0,81 1,1
    0,0068 0,0069
    1 1

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