PROCESS FLOW DIAGRAM PEMBUATAN ASAM

SITRAT BERBAHAN BAKU MOLASE

TK – 101 P – 101 R – 101 P – 102 C – 102 P – 103 F – 101 P – 104 E – 103 E – 104 EQ – 101 SE – 101 SE – 102 CR – 101
E – 101 E – 102 C – 101 V – 101 V – 102 C – 103
Mixing Tank Centrifuge FERMENTOR CLARIFIER Centrifuge Centrifuge Centrifuge Filter Pump Evaporator Rotary Conveyor Vibrating Vibrating Grinder
Heater Cooler Tank Tank Purification
FEED Pump Overflow Press Dryer Screen Screen
Netralitation Acidification Column
Pump Pump
8
c

H2SO4 98%
1'
c

Air
7
Ca(OH)2 Gas Out
6 21
Buffer 14 Vapor Out

5
Microba
130
1
4 Vapor Out
Nutrien 30
1
cc

E- 103 23
3 E - 101 E - 102 V
22

Water
11
cc

E - 104
TK - 101 V - 101 V - 102
CW v

30
1
R - 101
24
15 19 90
1
9 17
EQ - 101
P - 101 13
16
18 20
2 27
Molase
25
C - 101 C - 102 P - 103 26
C - 103
1
Air P - 102 SE - 101

12 18' 26' CR - 101

Carbon Activ 10
SE - 102 28
Citric Acid
F - 101 P - 104 Crystal 95%
29
CaSO4 dan H2S
O4

30
H2 O

Slurry
 4
Water 26ᵒC
Water

Molase 26ᵒC 3 9
Glucose 62%
Impurities13%
Water 25 % Molase
Glucose 62%
Impurities13%
2
Water 25 %
 Medium Medium
Sterilized Sterilized
100ᵒC 26ᵒC

Air pendingin Air pendingin

25ᵒC Bekas
50ᵒC
 Ca(OH)2
7
26ᵒC

(Liquid Phase) 30ᵒC 15

Asam sitrat
Water
Asam Oksalat

16 Product :
Steam in Water
Asam sitrat Steam Out
150ᵒC 90ᵒC Asam Oksalat 100ᵒC
Ca(OH)2
Kalsium Oksalat
Kalsium Sitrat
 Microba

Microba 2%
Microba 26ᵒC
Total Medium
CO2 CO2 (Gas Out)
N2 3 N2
02 30ᵒC 14 02
Udara 26ᵒC
Sterilized Medium
Sterilized Medium
Asam sitrat 30ᵒC
26ᵒC Asam Oksalat 11
Molase Nutrient
Molase Air
Glucose 62% Mikroba
Impurities 13% Impurities
Water 25 % Glukosa Asam sitrat
1 Asam Oksalat
Air
Nutrient Air Mikroba
Air Pendingin bekas Impurities
Air Pendingin 13 Glukosa
25ᵒC 28ᵒC
 13

Over Head (Liquid Phase)

Asam sitrat
Water
Asam Oksalat

15

Slurry :
10 Glucose
Microba
Impuritis
 13

Over Head (Liquid Phase)

Asam sitrat
Water
Asam Oksalat

15

Slurry :
10 Glucose
Microba
Impuritis
 18

Carbon Activ

12

Buffer
18' Water
Asam sitrat
Karbon Aktif
H2SO4 Kalsium Sulfat
 18'

Water
Asam sitrat
19

Karbon Aktif
H2SO4
Kalsium Sulfat
29
 21
Water Vapor

22

19 Asam sitrat 97,97 %

Recycle
20
-Asam sitrat 98%
 Udara
1'

Water
Asam sitrat 97,97 % Vapor out

22 23

Asam sitrat 98%

Water 2%
24
26' Asam sitrat 98%
Water 2%

28

Asam sitrat 98%

Water 2%

To Recycle
20
 10 m

6m
 D

Ht tk = 2D

H total