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Nguyn tc: tin hnh thy phn acid chuyn dng ng kh thnh ng
khng kh, sau tin hnh xc nh ng kh theo phng php chun iod.
Tin hnh:
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nghin k thnh dng ng th. Cho 20ml nc ct vo ci, nghin tip, lng, cht ly
phn nc vo cc. Sau lp li qu trnh trn 3 ln, dng nc ct trng li ci, chy s.
Chuyn ton b dch mu sang bnh nh mc (100ml), dng nc ct a th tch n
vch. Lc dch chit qua bng, c dch trit trong xc nh ng kh.
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Chuyn dng ng khng kh thnh ng kh: Ly 5ml trong 100ml dch chit
ng thm vo 2ml HCL 6N. t trn bp cch thy nhit 70 80oC trong thi gian
20 pht. Thnh thong lc u, cc ng kp c thy phn thnh ng n. Sau
khi ngui cho vo bnh 3 git phenolphtalein 1% trong cn 96o. Trung ha lng acid
cn d bng dung dch NaOH 10% cho n khi c mu hng. Lm chua li bng dung dch
CH3COOH 10% cho n khi mt mu. Dng nc ct ln th tch n vch, c dung
dch ng kh.
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thnh Fe2+ .
K3Fe(CN)6 + ng kh
K2Zn3[Fe(CN)6]2 + 3K2SO4
K4Fe(CN)6 + I2
Na2S4O6 + 2NaI
Chun bng Na2S2O3 0.05N cho n khi c mu vng rm. Thm 3 git
tinh bt (dung dch chuyn mu xanh), chun tip cho n khi c mu trng sa
hon ton.
Ch : nu sau khi cho (KI + ZnSO4) m dung dch c mu trng sa
ngay, c ngha l lng ng trong dung dch qu nhiu, cn phi lm li vi
lng mu t hn.
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nh lng ng tng s
0ml
0.00
0.00
-
0.10
1.15
0.20
-
0.30
-
1.00
1.50
1.67
1.83
2.00
2.00
3.00
4.00
5.00
6.00
3.10
4.72
6.37
8.06
9.72
3.26
4.88
6.54
8.22
9.89
3.24
5.64
6.71
8.39
10.06
3.58
5.20
6.88
8.56
10.23
0.40
2016.
00
3.74
5.36
7.05
8.72
10.41
0.50
0.73
0.60
0.87
0.70
1.02
0.80
1.18
0.90
1.34
2.13
2.47
2.62
2.78
2.94
3.90
5.53
7.22
8.89
10.58
4.06
5.70
7.39
9.06
10.75
4.22
5.86
7.55
9.22
10.92
4.38
6.03
7.72
9.39
11.10
4.54
6.20
7.80
9.55
11.28
7.00
8.00
9.00
11.46
13.28
14.99
11.64
13.46
-
11.82
13.63
-
12.00
13.80
-
12.18
13.97
-
12.36
14.14
-
12.54
14.31
-
12.73
14.49
-
12.91
14.66
-
13.10
14.83
-